This book is well written, easy to read and contains information from multiple resources for the benefit of students. All the methods explained in this book are easy to learn as it presents clearly drawn diagrams and text written in a simple language. This book is written strictly following the new syllabus of Seventh Semester BPharm regulated by Pharmacy Council of India (PCI), and BSc and MSc (analytical chemistry) courses. It will prove useful to both the students as well as the teachers. The systematic structure of the book is assigned to cover the major syllabi of instrumental methods of analysis in V units (19 chapters), includes all topics of syllabus and basic experiments.