Pharmaceutical Analysis is a branch of practical chemistry that involves identification, determination, quantification and purification of a compound, separation of the components of a solution or mixture, or determination of structure of chemical compounds. So, considering plethora of application and wide utility of pharmaceutical analysis in pharmaceutical sciences, "Pharmaceutical Analysis: A Practical Manual" was designed. This manual consists of different chapters dealing with the detailed information of pharmaceutical analytical techniques and organized according to the type of titration or techniques. Each technique is explained along with the experiments. One section of the manual is designed for the titration techniques involved in pharmaceutical analysis whereas another section deals with electrophoresis and chromatography techniques. This manual will suffice the requirements of academics and research. Moreover, this manual can be treated as reference for pharmaceutical analytical techniques.